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This is an atmosphere-controlled box furnace, which is designed for sintering materials under high purity oxygen. The furnace consists of high-quality alumina fiber bricks and MoSi2 heating elements with a heating chamber of 8″x 8″x8″. It is an ideal tool for preparing high purity oxide ceramic materials, especially for high Ni battery cathode materials.
This is an atmosphere-controlled box furnace, which is designed for sintering materials under high purity oxygen. The furnace consists of high-quality alumina fiber bricks and MoSi2 heating elements with a heating chamber of 8″x 8″x8″. It is an ideal tool for preparing high purity oxide ceramic materials, especially for high Ni battery cathode materials. The furnace also can be used under inert gases up to 1600oC.
SPECIFICATIONS
| Furnace structure | MoSi2 heating elements with Ni coated copper capable connection
Double-layer steel structure for maximum vacuum and safety. Water cooling front door and air cooling shell Built-in pressure gauge, vacuum valves, and two gas float meters |
| Power | AC 208 – 240V single phase (50/ 60 Hz)
30 Amp (50 Amp air breaker is required) 7.5 KW The power cable is included but no plug ( please inform us of your plug type, we can install for you upon request |
| Heating Elements | 6 sets of MoSi2 heating elements are built-in and replaceable
Working temperature range: 1200oC – 1700oC in air or oxygen Note: the heating elements also can be used under inert gas at 1000oC – 1600 oC) The furnace is not a high vacuum furnace. The vacuum level is about 500 torr at high temperature |
| Temperature | Continuous 300 – 1600°C
Max. 1700°C(<60min) Accuracy: +/- 0.1°C Heating Rate: 5°C / min Thermocouple: two B type T/C for control and monitor alarm separately |
| Control Panel | Built-in PC for controlling temperature and pressure
Temperature Control: Eurotrem 3000 controllers inside for +/- 0.1oC accuracy connected to PC 24 segments programmable Protection for over-temperature and current, as well as the thermal couple, broke A secondary temperature controller is built-in for extra over-temperature protection. Pressure Control: The pressure sensor and pressure controller are installed to control the set pressure constant. The pressure control can be used to perform the following functions: Inert gas Purging via manually or an automatic mode Constand pressure during heating High and Low-pressure protection The pressure controllable range: -0.06 to 0.03Mpa. Safety Alarm System: Over-temperature protection Over-pressure and lower pressure alert Low water flow alert Data Collection Recording temperature profile Recording pressure profile All data is saved to the hard disc of the PC |
| Vacuum pump & Gas Flow Control | Two large flow meters are installed on the front panel of the furnace for purging via inert gas and filling oxygen gases
One vacuum pump is included to enhance purging and keep the chamber below 760 torr Low vacuum 10-1 torr due to fibrous alumina insulation material. Using 5% H2 + Ar will improve oxidation during heating. For oxygen-sensitive material, please use a hydrogen furnace |
| Water Cooling | A 58L/min recirculating water cooling is required to cool the furnace sealing flange and chamber case. |